Low molecular weight MPEG-assisted organic synthesis

Figlus, M., Tarruella, A.C., Messer, A., Sollis, S.L. and Hartley, R.C. (2010) Low molecular weight MPEG-assisted organic synthesis. Chemical Communications, 46(24), pp. 4405-4407. (doi:10.1039/c0cc00415d)

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Publisher's URL: http://dx.doi.org/10.1039/c0cc00415d

Abstract

A toolkit of low molecular weight MPEG-supported coupling agents (<sup>M</sup>IIDQ, <sup>M</sup>EDCI), reagents for the Mitsunobu reaction (<sup>M</sup>DEAD, <sup>M</sup>TPP), an alternative to diazomethane, and scavengers can be used in the solution-phase synthesis of amides, esters and ureas and are easily removed after use by solid-phase extraction (MSPE) using normal silica.

Item Type:Articles
Status:Published
Refereed:Yes
Glasgow Author(s) Enlighten ID:Hartley, Professor Richard and Figlus, Mr Marek
Authors: Figlus, M., Tarruella, A.C., Messer, A., Sollis, S.L., and Hartley, R.C.
Subjects:Q Science > QD Chemistry
College/School:College of Science and Engineering > School of Chemistry
Journal Name:Chemical Communications
Journal Abbr.:Chem. Comm.
Publisher:Royal Society of Chemistry
ISSN:1359-7345
ISSN (Online):1364-548X
Published Online:14 May 2010

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Project CodeAward NoProject NamePrincipal InvestigatorFunder's NameFunder RefLead Dept
479311Light MPEG supports for the synthesis of arraysRichard HartleyEngineering & Physical Sciences Research Council (EPSRC)EP/F068174/1Chemistry