Blake, A.J., Caltagirone, C., Lippolis, V., Schröder, M. and Wilson, C. (2004) (Ferrocenylmethyl)trimethylammonium triiodide. Acta Crystallographica. Section E: Structure Reports Online, 60(1), m20-m21. (doi: 10.1107/s1600536803026084)
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Abstract
The salt (ferrocenylmethyl)trimethylammonium iodide, [Fe(C5H5)(C9H15N)]I, is used in an established procedure to attach ferrocenylmethyl frameworks to secondary amines. The title salt, [Fe(C5H5)(C9H15N)]I3, obtained by diffusion of Et2O vapour into a CH2Cl2 solution containing equimolar [Fe(C5H5)(C9H15N)]I and I2, shows the expected cation balanced by an asymmetric but isolated triiodide counteranion [I-I = 3.0006 (4) and 2.8728 (4) Å].
Item Type: | Articles |
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Status: | Published |
Refereed: | Yes |
Glasgow Author(s) Enlighten ID: | Wilson, Dr Claire |
Authors: | Blake, A.J., Caltagirone, C., Lippolis, V., Schröder, M., and Wilson, C. |
College/School: | College of Science and Engineering > School of Chemistry |
Journal Name: | Acta Crystallographica. Section E: Structure Reports Online |
Publisher: | International Union of Crystallography |
ISSN: | 1600-5368 |
Published Online: | 12 December 2003 |
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