Chambers, O. R., Harman, M. E., Rycroft, D. S., Sharp, D. W.A. and Winfield, J. M. (1977) Alkylimidotungsten(VI) fluorides. Journal of Chemical Research(6), (S) 150-151-(M) 1849-1876.
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Abstract
Although a number of transition-metal compounds containing terminal alkylimido-ligands are known, <sup>1</sup>H—<sup>14</sup>N spin—spin coupling has apparently not been observed in their n.m.r. spectra. We report the preparation and characterisation of several alkylimido-derivatives of tungsten hexafluoride in which spin—spin coupling interactions involving <sup>14</sup>N are observed. The observation of n.m.r. parameters involving <sup>14</sup>N enables structural assignments to be made.
Item Type: | Articles |
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Keywords: | NMR spectroscopy. |
Status: | Published |
Refereed: | Yes |
Glasgow Author(s) Enlighten ID: | Winfield, Professor John and Rycroft, Dr David |
Authors: | Chambers, O. R., Harman, M. E., Rycroft, D. S., Sharp, D. W.A., and Winfield, J. M. |
Subjects: | Q Science > QD Chemistry |
College/School: | College of Science and Engineering > School of Chemistry |
Journal Name: | Journal of Chemical Research |
Publisher: | The Chemical Society |
ISSN: | 0308-2342 |
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