Miras, H.N. , Woollins, J.D., Slawin, A.M., Raptis, R., Baran, P. and Kabanos, T.A. (2003) A novel polyoxo(thio)molybdenum(V) sulfite compound: Synthesis and crystal structure of {Mo-2(V)(mu-S)(2)O-2](6)(mu(3)-SO3)(4)(mu-SO3)(12)}(20-)anion. Dalton Transactions(19), pp. 3668-3670. (doi: 10.1039/B309473C)
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Abstract
The non-cyclic polyoxo(thio) molybdate(V)-sulfite K-6(NH4)(14){Mo-2(V)(mu-S)(2)O-2](6)(mu(3)-SO3)(4)(mu-SO3)(12)} . 7H(2)O 1 was prepared by self-condensation of Mo-2(V)(mu-S)(2)O-2](2+) building block in the presence of (NH4)(2)SO3. Compound 1 was characterized by X-ray structure analysis as well as IR, UV-vis spectroscopies and thermogravimetric analysis.
| Item Type: | Articles |
|---|---|
| Status: | Published |
| Refereed: | Yes |
| Glasgow Author(s) Enlighten ID: | Moiras, Professor Haralampos |
| Authors: | Miras, H.N., Woollins, J.D., Slawin, A.M., Raptis, R., Baran, P., and Kabanos, T.A. |
| College/School: | College of Science and Engineering > School of Chemistry |
| Journal Name: | Dalton Transactions |
| Publisher: | Royal Society of Chemistry |
| ISSN: | 1477-9226 |
| ISSN (Online): | 1477-9234 |
| Published Online: | 21 August 2003 |
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