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Frampton, C.S., Gall, J.H., and MacNicol, D.D. (2000) Hexabenzylbenzene. Acta Crystallographica. Section C: Crystal Structure Communications, 56 (1). e22-e23. ISSN 0108-2701 (doi:10.1107/S0108270199016005)
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Publisher's URL: http://dx.doi.org/10.1107/S0108270199016005
Abstract
The title compd. crystallizes unsolvated in triclinic space group P1 (a 8.999(2), b 10.456(4), c 10.622(4) , a 69.218(12), b 79.20(2), g 67.07(2), Z = 1, dc = 1.196, R = 0.038, Rw(F2) = 0.111 for 3460 reflections) and a centrosym. ababab conformation (a and b denote side-chain units projecting, resp., above and below the plane of the arom. core), which possesses noncrystallog. 3 (S6) symmetry. The CH2 C atoms, in cyclic order, deviate from the mean plane of the central benzene ring by 0.042, -0.029, 0.050, -0.042, 0.029 and -0.050 (root-mean-square deviation 0.041).
| Item Type: | Article |
|---|---|
| Status: | Published |
| Refereed: | Yes |
| Glasgow Author(s): | Gall, Mr James and MacNicol, Dr David |
| Authors: | Frampton, C.S., Gall, J.H., and MacNicol, D.D. |
| Subjects: | Q Science > QD Chemistry |
| College/School: | College of Science and Engineering > School of Chemistry |
| Journal Name: | Acta Crystallographica. Section C: Crystal Structure Communications |
| Publisher: | Wiley-Blackwell Publishing, Inc. |
| ISSN: | 0108-2701 |
| ISSN (Online): | 1600-5759 |
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