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2,2,4,4-Tetramethyl-1,5-diphenyl-6,7,8-trioxa-3- thiabicyclo[3.2.1]-octane

Cuthbertson, E., Frampton, C.S., and MacNicol, D.D. (2000) 2,2,4,4-Tetramethyl-1,5-diphenyl-6,7,8-trioxa-3- thiabicyclo[3.2.1]-octane. Acta Crystallographica. Section C: Crystal Structure Communications, 56 (12). pp. 1510-1511. ISSN 0108-2701 (doi:10.1107/S0108270100013147)

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Publisher's URL: http://dx.doi.org/10.1107/S0108270100013147

Abstract

The structure of the title ozonide, C20H22O3S, produced without the use of ozone, has been defined at 123 (1) K. In the triclinic crystal, the molecule has symmetry close to Cs, and its ozonide and 1,4-oxathiane rings have envelope and chair conformations, respectively. The ozonide unit has an O-O bond length of 1.4721 (12) Angstrom and a C-O-O-C torsion angle of - 1.45 (12)degrees.

Item Type:Article
Status:Published
Refereed:Yes
Glasgow Author(s):MacNicol, Dr David
Authors: Cuthbertson, E., Frampton, C.S., and MacNicol, D.D.
Subjects:Q Science > QD Chemistry
College/School:College of Science and Engineering > School of Chemistry
Journal Name:Acta Crystallographica. Section C: Crystal Structure Communications
Publisher:Wiley-Blackwell Publishing, Inc.
ISSN:0108-2701
ISSN (Online):1600-5759

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