The nuclear magnetic resonance spectra of geometrical isomers of 2,4-difluoro-1,3- di-t-butylcyclodiphosph(III)azane

Keat, R., Rycroft, D. S., Niecke, E., Schäfer, H.-G. and Zorn, H. (1982) The nuclear magnetic resonance spectra of geometrical isomers of 2,4-difluoro-1,3- di-t-butylcyclodiphosph(III)azane. Zeitschrift für Naturforschung B - A Journal of Chemical Sciences, 37(12), pp. 1665-1666. (doi:10.1515/znb-1982-1234)

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Abstract

A new synthetic method for the preparation of the geometrical isomers of (FPNBut)2 by amine elimination from Me2N–P(F)–NButSiMe2 is described. The 13C, 19F, and 31P NMR investigations lead to new structural assignments.

Item Type:Articles
Keywords:Phosphorus chemistry, NMR spectroscopy.
Status:Published
Refereed:Yes
Glasgow Author(s) Enlighten ID:Rycroft, Dr David
Authors: Keat, R., Rycroft, D. S., Niecke, E., Schäfer, H.-G., and Zorn, H.
Subjects:Q Science > QD Chemistry
College/School:College of Science and Engineering > School of Chemistry
Journal Name:Zeitschrift für Naturforschung B - A Journal of Chemical Sciences
Publisher:Verlag der Zeitschrift für Naturforschung
ISSN:0340-5087
Copyright Holders:Copyright © 1982 Verlag der Zeitschrift für Naturforschung
First Published:First published in Zeitschrift für Naturforschung B - A Journal of Chemical Sciences 37(12): 1665-1666
Publisher Policy:Reproduced under a Creative Commons License

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